Direct Investigation of Synthesis of Gold Nanoparticles Using Polyscias Scutellaria Leaf Extract in the Hexane-Water System Using the Centrifugal Liquid Membrane-Spectrophotometry Method

Kurniawan, Muhammad Rizki and Humaedi, Aji and Ritonga, Ahmad Fitra (2020) Direct Investigation of Synthesis of Gold Nanoparticles Using Polyscias Scutellaria Leaf Extract in the Hexane-Water System Using the Centrifugal Liquid Membrane-Spectrophotometry Method. Jurnal Kimia Sains dan Aplikasi, 23 (7). pp. 255-260. ISSN 1410-8917

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Abstract

The Centrifugal liquid Membrane (CLM) method, which provides an ultra-thin two-phase liquid membrane system in a rotating glass cell, was successfully applied to Green Synthesis from Polyscias Scutellaria (PS) capped gold nanoparticles (AuNPs-PS) using a Mangkokan leaf (Polyscias Scutellaria) extract as a reducing agent and stabilizer in the hexane-water system. PS extract in hexane fraction as the organic phase has a UV absorption spectrum at the maximum wavelength, λmax of 220 nm, while the precursor of HAuCl4 solution as an aqueous phase has an λmax of 214 nm. Investigation of AuNPs-PS formation was carried out at various concentrations of Mangkokan leaf extract concentration; i.e., 0.001 0.003; 0.005; 0.007 and 0.009%, while the reaction was carried out at various rotational speeds of 5,000-9,000 rpm. The formation and stability of AuNPs-PS were observed from the phenomenon of surface plasmon resonance (SPR) and absorbance changes as measured by a UV-Vis spectrophotometer. The results of measurements using CLM-Spectrophotometry shows the formation of AuNPs-PS in the hexane-water system at λmax of 534 nm.

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